Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid
CAS No.:92070-32-1
Molecular Formula:C₅₇H₇₀N₂O₂₄
Molecular Weight:1167.18
Hs Code.:

Benzyl-O-<methyl-(4,5,7,8-tetra-O-acetyl-3-desoxy-β-D-manno-2-octulopyranosyl)onat>-(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

There total 8 articles about Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.3%

: 108-24-7
acetic anhydride

: 92052-22-7,92052-23-8
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: In pyridine; at 0 ℃; for 18h;

Reference yield: 1.3%

: 108-24-7
acetic anhydride

: 92052-22-7,92052-23-8
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: In pyridine; at 0 ℃; for 18h;

Reference yield:

: 92052-20-5
Benzyl-6-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

: 92070-32-1,92125-37-6
Benzyl-O--(2->3)-O-(2-acetamido-2-desoxy-4,6-O-ethyliden-β-D-glucopyranosyl)-(1->6)-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: Hg(CN)2, molecular sieve (4 Angstroem) / nitromethane / 1.) 60 deg C, 2 h, 2.) room temp., 18 h

2: 13 percent / pyridine / 18 h / 0 °C

With 4 A molecular sieve; mercury(II) cyanide; In pyridine; nitromethane;