N-methyl o-(triphenylphosphoranylidene)amino benzamide

Base Information

• Chemical Name: N-methyl o-(triphenylphosphoranylidene)amino benzamide
• CAS No.: 118988-18-4
• Molecular Formula: C₂₆H₂₃N₂OP
• Molecular Weight: 410.455
• Mol file: 118988-18-4.mol

Synonyms:

Chemical Property of N-methyl o-(triphenylphosphoranylidene)amino benzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-methyl o-(triphenylphosphoranylidene)amino benzamide

There total 1 articles about N-methyl o-(triphenylphosphoranylidene)amino benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-Methyl-o-azido-benzamid (32709-38-9) + triphenylphosphine (603-35-0) → N-methyl o-(triphenylphosphoranylidene)amino benzamide (118988-18-4)

Guidance literature:

In diethyl ether; dichloromethane; for 3h; Ambient temperature;

DOI:10.1016/S0040-4020(01)81321-1

Reference yield: 98.0%

p-chlorphenylisocyanate (104-12-1) + N-methyl o-(triphenylphosphoranylidene)amino benzamide (118988-18-4) → 2-(p-chlorophenyl)amino-3-methyl-4(3H)-quinazolinone (118988-22-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)82131-0

Reference yield: 96.0%

N-methyl o-(triphenylphosphoranylidene)amino benzamide (118988-18-4) + 4-Methoxyphenyl isocyanate (5416-93-3) → 2-(p-methoxyphenyl)amino-3-methyl-4(3H)-quinazolinone (118988-21-9)

Guidance literature:

DOI:10.1016/S0040-4039(00)82131-0

upstream raw materials:

N-Methyl-o-azido-benzamid

triphenylphosphine

Downstream raw materials:

3-methyl-2,4(1H,3H)-quinazolinedione

2-(p-chlorophenyl)amino-3-methyl-4(3H)-quinazolinone

1,3-Bis-(4-chloro-phenyl)-1-{4-[(Z)-methylimino]-4H-benzo[d][1,3]oxazin-2-yl}-urea

1-{4-[(Z)-Methylimino]-4H-benzo[d][1,3]oxazin-2-yl}-1,3-diphenyl-urea