6-bromo-1,4-dimethyl-9H-carbazole

Base Information

• Chemical Name: 6-bromo-1,4-dimethyl-9H-carbazole
• CAS No.: 69902-42-7
• Molecular Formula: C₁₄H₁₂BrN
• Molecular Weight: 274.16
• DSSTox Substance ID: DTXSID50403981
• Nikkaji Number: J362.831K
• Wikidata: Q82207908
• Mol file: 69902-42-7.mol

Synonyms:6-bromo-1,4-dimethyl-9H-carbazole;69902-42-7;SCHEMBL6828975;DTXSID50403981;MFCD04124810;AKOS005084480;1X-0836;A923559

Chemical Property of 6-bromo-1,4-dimethyl-9H-carbazole

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 273.01531
• Heavy Atom Count: 16
• Complexity: 268

Purity/Quality:

97% ^*data from raw suppliers

6-Bromo-1,4-dimethyl-9H-carbazole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C2C3=C(C=CC(=C3)Br)NC2=C(C=C1)C

Technology Process of 6-bromo-1,4-dimethyl-9H-carbazole

There total 8 articles about 6-bromo-1,4-dimethyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5-bromo-1H-indole (10075-50-0) + 2,5-hexanedione (110-13-4) → 6-bromo-1,4-dimethyl-9-H-carbazole (69902-42-7)

Guidance literature:

montmorillonite K-10; at 90 ℃; for 0.05h; microwave heating;

DOI:10.1002/adsc.200606200

Reference yield: 52.0%

5-bromo-1H-indole (10075-50-0) + hexane-2,5-diol (2935-44-6) → 6-bromo-1,4-dimethyl-9-H-carbazole (69902-42-7)

Guidance literature:

With montmorillonite K-10; at 160 ℃; for 1h; Microwave irradiation; neat (no solvent);

DOI:10.1055/s-0029-1217052

Reference yield: 39.0%

N-[N-(4-bromophenyl)-N-(2,5-dimethylphenyl)amino]phthalimide (288264-28-8) → 1,4-dimethyl-9H-carbazole (18028-55-2) + 6-bromo-1,4-dimethyl-9-H-carbazole (69902-42-7)

Guidance literature:

With aluminium trichloride; In benzene; at 20 ℃; for 4h;

DOI:10.1021/jo016124r

upstream raw materials:

N-[N-(4-bromophenyl)-N-(2,5-dimethylphenyl)amino]phthalimide

5-bromo-1H-indole

2,5-hexanedione

1.4-dibromobenzene

Downstream raw materials:

3-amino-1,4-dimethyl-9H-carbazole

9-bromoellipticine

6-bromo-1,4-dimethyl-9-H-carbazole-3-carbaldehyde

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