Phenol, 2,4,6-trichloro-, thallium(1+) salt

Base Information

Chemical Name:Phenol, 2,4,6-trichloro-, thallium(1+) salt
CAS No.:120868-76-0
Molecular Formula:C6H3Cl3O.Tl
Molecular Weight:400.823
Hs Code.:
Mol file:120868-76-0.mol

Synonyms:

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Chemical Property of Phenol, 2,4,6-trichloro-, thallium(1+) salt

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Technology Process of Phenol, 2,4,6-trichloro-, thallium(1+) salt

There total 2 articles about Phenol, 2,4,6-trichloro-, thallium(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 20398-06-5
thallium (I) ethoxide

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 120868-76-0
thallium(I) 2,4,6-trichlorophenoxide

Guidance literature:: In ethanol; heating; elem. anal.;
DOI:10.1016/0022-328X(88)80389-9

Reference yield: 68.0%

: thallium(I) nitrate

: 88-06-2,67471-29-8
2,4,6-Trichlorophenol

: 120868-76-0
thallium(I) 2,4,6-trichlorophenoxide

Guidance literature:: With KOH; In methanol; water; MeOH soln. of C6H2Cl3OH stirred with aq. KOH; aq. soln. of TlNO3 added; heated to reflux for 3 h; allowed to evaporate for several d; elem. anal.;
DOI:10.1002/zaac.201100114

Reference yield: 37.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 120868-76-0
thallium(I) 2,4,6-trichlorophenoxide

: mercury dibromide

: 120868-75-9
bis(2,4,6-trichlorophenoxymethyl)mercury

Guidance literature:: In tetrahydrofuran; diethyl ether; addn. of diazomethane (ether) to HgBr2 in ether, (BrH2C)2Hg formed "in situ", filtered solution added to TlOC6H2Cl3(THF), stirring overnight at 30-40°C; washed with cold 95% ethanol;
DOI:10.1016/0022-328X(88)80389-9