{21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride

Base Information

Chemical Name:{21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride
CAS No.:96326-86-2
Molecular Formula:C₅₁H₃₄Cl₉FeN₄O
Molecular Weight:1093.78
Hs Code.:

Synonyms:

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Chemical Property of {21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride

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Technology Process of {21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride

There total 2 articles about {21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91042-27-2,186099-12-7
5,10,15,20-tetra(2',6'-dichlorophenyl)porphyrinatoiron(III) chloride

: 762-62-9
4,4-dimethylpent-1-ene

: 96326-86-2
{21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride

Guidance literature:: With 1,2,3,4,5-pentafluoro-6-iodosylbenzene; In dichloromethane; dissolving of (tetrakis(2.6-dichlorophenyl)porphinato)iron chloride (0.010 mmol) and 4,4-dimethyl-1-pentene (2.6 mmol) with stirring in CH2Cl2; addn. of pentafluoroiodosylbenzene (1.2 mmol); evaporation to dryness on a rotary evaporator;; drying under vac. (<1 Torr) for 20 h; dissolving in CH2Cl2; spotting on a silica gel glass plate and developing (CH3OH/CH2Cl2); extraction of the green band with CH3OH/CH2Cl2; filtration; evaporation to dryness; recrystallization from CH2Cl2/hexane;;
DOI:10.1021/ja00246a019

Reference yield:

: 96326-85-1
{21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}aquoiron(III) chloride

: 14353-90-3
1,2,3,4,5-pentafluoro-6-iodosylbenzene

: 96326-86-2
{21-(4,4-dimethyl-2-oxidopentyl)-5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato}iron(III) chloride

Guidance literature:: With hydrogenchloride; In dichloromethane; water; Fe-complex in CH2Cl2 had been previously treated with aq. HCl was treated with iodosopentafluorobenzene;
DOI:10.1021/ja00298a064