triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

Base Information

Chemical Name:triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide
CAS No.:860453-03-8
Molecular Formula:C₂₄H₂₄AuOP
Molecular Weight:556.394
Hs Code.:

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Chemical Property of triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

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Technology Process of triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

There total 1 articles about triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 860452-97-7
gold 3-hydroxy-3-methyl-1-pentynylide

: 603-35-0
triphenylphosphine

: 860453-03-8
triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

Guidance literature:: In toluene; (N2); soln. of P ligand (1 equiv.) in toluene was added to suspn. of Au compd. (1 equiv.) in toluene; mixt. was stirred for 5-10 min; filtered; solvent removed (vac., 50°C); recrystd. (toluene/heptane); elem. anal.;
DOI:10.1016/j.jorganchem.2005.02.045

Reference yield: 37.3%

: 860453-03-8
triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

: [Me₄N][nido-7,8-As₂B₉H₁₀]

: 889128-90-9
[Me₄N][3-(PPh₃)-closo-3,1,2-AuAs₂B₉H₉]

Guidance literature:: In ethanol; acetone; Au complex added to suspn. of B compd. in EtOH-acetone; heated at refluxfor 2.5 h; filtered; solvent removed from filtrate under reduced pressure (50°C); crystd. from CH2Cl2-hexane; elem. anal.;
DOI:10.1039/b515165a

Reference yield: 20.0%

: 860453-03-8
triphenylphosphine gold 3-hydroxy-3-methyl-1-pentynylide

: [Et₄N][nido-TeB₁₀H₁₁]

: [Et₄N][2-(PPh₃)-closo-2,1-AuTeB₁₀H₁₀]

Guidance literature:: In ethanol; acetone; Au complex added to suspn. of B compd. in EtOH-acetone; heated at refluxfor 4 h; cooled to room temp.; filtered; solvent removed from filtrate by rotary evaporator (50°C); crystd. from CH2Cl2; elem. anal.;
DOI:10.1039/b515165a