(methyl-4 phenyl)-3 butanedithioate de methyle

Base Information

• Chemical Name: (methyl-4 phenyl)-3 butanedithioate de methyle
• CAS No.: 70369-25-4
• Molecular Formula: C₁₂H₁₆S₂
• Molecular Weight: 224.391
• Mol file: 70369-25-4.mol

Synonyms:

Chemical Property of (methyl-4 phenyl)-3 butanedithioate de methyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (methyl-4 phenyl)-3 butanedithioate de methyle

There total 6 articles about (methyl-4 phenyl)-3 butanedithioate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(methyl-4 phenyl)-3 N-phenyl butanimidothioate de methyle (95503-02-9) → (methyl-4 phenyl)-3 butanedithioate de methyle (70369-25-4)

Guidance literature:

With hydrogen sulfide; trifluoroacetic acid; In N,N-dimethyl-formamide; for 18h; Yield given;

Reference yield:

N-phenyl butene-3 imidothioate de methyle (121726-26-9) → (methyl-4 phenyl)-3 butanedithioate de methyle (70369-25-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 5 percent DBU / tetrahydrofuran / 16 h / Heating

2: 75 percent / tetrahydrofuran / 2 h / -10 - -5 °C

3: trifluoroacetic acid, H₂S / dimethylformamide / 18 h

With hydrogen sulfide; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

N-phenyl butene-2 imidothioate de methyle (65672-29-9,95502-91-3,121726-25-8) → (methyl-4 phenyl)-3 butanedithioate de methyle (70369-25-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 °C / 0.4 Torr

2: 75 percent / tetrahydrofuran / 2 h / -10 - -5 °C

3: trifluoroacetic acid, H₂S / dimethylformamide / 18 h

With hydrogen sulfide; trifluoroacetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

upstream raw materials:

(methyl-4 phenyl)-3 N-phenyl butanimidothioate de methyle

N-phenyl butene-3 imidothioate de methyle

N-phenyl butene-2 imidothioate de methyle

(E)-N-phenyl butene-2 imidothioate de methyle