1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

Base Information

Chemical Name:1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide
CAS No.:135396-31-5
Molecular Formula:C₃₂H₂₀N₆O₅
Molecular Weight:568.548
Hs Code.:

Synonyms:

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Chemical Property of 1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

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Technology Process of 1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

There total 6 articles about 1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 135396-30-4
6-amino-1,3-diphenyl-5-nitrosouracil

: 135396-32-6
4,6-diphenylfurazano<3,4-d>pyrimidine-5,7(4H,6H)-dione

: 135396-31-5
1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

Guidance literature:: With lead(IV) acetate; In acetic acid; for 0.5h; Mechanism; Ambient temperature; other uracils;
DOI:10.1021/jo00022a017

Reference yield:

: 102-07-8
bis(diphenyl)urea

: 135396-31-5
1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: acetic anhydride / 4.5 h / 90 - 100 °C / Inert atmosphere

2: trichlorophosphate / water / 3.33 h / 0 - 110 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5: sodium nitrite / water; acetic acid / 1 h / 0 - 20 °C / Inert atmosphere

6: lead(IV) tetraacetate / acetic acid / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; lead(IV) tetraacetate; sodium nitrite; trichlorophosphate; In tetrahydrofuran; water; acetic anhydride; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/chem.201900118

Reference yield:

: 5759-74-0
6-chloro-1,3-diphenyluracil

: 135396-31-5
1,3,6,8-tetraphenylpyrimido<5,4-g>pteridine-2,4,5,7(1H,3H,6H,8H)-tetrone 10-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3: sodium nitrite / water; acetic acid / 1 h / 0 - 20 °C / Inert atmosphere

4: lead(IV) tetraacetate / acetic acid / 1 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium azide; lead(IV) tetraacetate; sodium nitrite; In tetrahydrofuran; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/chem.201900118