2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

Base Information

Chemical Name:2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane
CAS No.:121124-95-6
Molecular Formula:C11H13BrO3
Molecular Weight:273.126
Hs Code.:
DSSTox Substance ID:DTXSID301277914
Mol file:121124-95-6.mol

Synonyms:2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane;121124-95-6;2-(3-Bromo-6-methoxyphenyl)-1,3-dioxane;SCHEMBL3686228;QYGXFNAOPHJOMY-UHFFFAOYSA-N;DTXSID301277914;2-(5-Bromo-2-methoxy-phenyl)-[1,3]dioxane

Suppliers and Price of 2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:272.00481
Heavy Atom Count:15
Complexity:194

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Br)C2OCCCO2

Technology Process of 2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

There total 1 articles about 2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 25016-01-7
5-bromo-2-methoxybenzaldehyde

: 504-63-2
trimethyleneglycol

: 121124-95-6
2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

Guidance literature:: With boron trifluoride diethyl etherate; In toluene; for 4h; Heating;

Reference yield:

: 121124-95-6
2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

: 121125-12-0
(S)-2-Benzyloxycarbonylamino-3-[3'-((S)-2-benzyloxycarbonyl-2-tert-butoxycarbonylamino-ethyl)-4-methoxy-biphenyl-3-yl]-propionic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

2: KOtBu / CH₂Cl₂ / 14 h / -60 - 20 °C

3: Irradiation

4: H₂ / (+) / methanol / 72 h / 20 °C

With potassium tert-butylate; hydrogen; (+); In methanol; dichloromethane;

Reference yield:

: 121124-95-6
2-(5-Bromo-2-methoxyphenyl)-1,3-dioxane

: 121141-61-5
(S)-2-Benzyloxycarbonylamino-3-[3'-((S)-2-benzyloxycarbonyl-2-tert-butoxycarbonylamino-ethyl)-4,4'-dimethoxy-biphenyl-3-yl]-propionic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

2: KOtBu / CH₂Cl₂ / 14 h / -60 - 20 °C

3: Irradiation

4: H₂ / (+) / methanol / 72 h / 20 °C

With potassium tert-butylate; hydrogen; (+); In methanol; dichloromethane;