Technology Process of 8-(2-Hydroxy-3,4-dimethoxy-6-methyl-phenyl)-8-oxo-octanoic acid
There total 1 articles about 8-(2-Hydroxy-3,4-dimethoxy-6-methyl-phenyl)-8-oxo-octanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide; aluminium trichloride;
Multistep reaction;
1.) nitrobenzene, 0 deg C, 6 h, RT, 64 h;
DOI:10.1248/cpb.30.2797
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) NaBH4, 2.) H2 / 2.) 5percent Pd/C / 1.) methanol, 2.) acetic acid, RT, 70 min. Other reagent: Zn/Hg
2: 78 percent / ON(SO3K)2, 1percent NaOH / H2O / 1 h / Ambient temperature
With
sodium hydroxide; sodium tetrahydroborate; potassium nitrososulfonate; hydrogen;
palladium on activated charcoal;
In
water;
DOI:10.1248/cpb.30.2797
- Guidance literature:
-
With
sodium tetrahydroborate; hydrogen;
palladium on activated charcoal;
Yield given. Multistep reaction;
1.) methanol, 2.) acetic acid, RT, 70 min. Other reagent: Zn/Hg;
DOI:10.1248/cpb.30.2797
