4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Base Information

Chemical Name:4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid
CAS No.:261724-19-0
Molecular Formula:C₄₁H₅₂N₂O₂₂
Molecular Weight:924.864
Hs Code.:

4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Synonyms:

Suppliers and Price of 4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

There total 6 articles about 4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 261724-38-3
4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid benzyl ester

: 261724-19-0
4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0968-0896(99)00226-6

Reference yield:

: 193156-91-1
[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethylamino]-acetic acid benzyl ester

: 261724-19-0
4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / DCC; HOBt; DIEA / CH₂Cl₂ / 16 h / 20 °C

2: H₂ / 10 percent Pd/C / ethanol

3: 97 percent / DIEA; HATU / CH₂Cl₂

4: H₂ / 10 percent Pd/C / ethanol

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium on activated charcoal; In ethanol; dichloromethane; 1: Acylation / 2: Hydrogenolysis / 3: Substitution / 4: Hydrogenolysis;
DOI:10.1016/S0968-0896(99)00226-6

Reference yield:

: 193156-89-7
2-(2,3,4,6-tetra-O-acetylated-1-deoxy-α-D-galactopyranosyl)-ethanoic acid

: 261724-19-0
4-(2-{[2-((2R,3S,4R,5S,6R)-3,4,5-Triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-acetyl]-[2-((2R,3S,4R,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yl)-ethyl]-amino}-acetylamino)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / DCC; HOBt; DIEA / CH₂Cl₂ / 16 h / 20 °C

2: H₂ / 10 percent Pd/C / ethanol

3: 97 percent / DIEA; HATU / CH₂Cl₂

4: H₂ / 10 percent Pd/C / ethanol

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; palladium on activated charcoal; In ethanol; dichloromethane; 1: Acylation / 2: Hydrogenolysis / 3: Substitution / 4: Hydrogenolysis;
DOI:10.1016/S0968-0896(99)00226-6