Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-

Base Information

Chemical Name:Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-
CAS No.:81025-25-4
Molecular Formula:C₁₆H₁₆
Molecular Weight:208.303
Hs Code.:
DSSTox Substance ID:DTXSID001131638

Synonyms:DTXSID001131638;81025-25-4;Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-

Suppliers and Price of Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:208.125200510
Heavy Atom Count:16
Complexity:345

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2C=CC1C3(CC3C4=CC=CC=C4)C=C2

Technology Process of Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]-

There total 2 articles about Spiro[bicyclo[3.2.1]octa-3,6-diene-2,1'-cyclopropane], 2'-phenyl-, [1alpha,2beta(S*),5alpha]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 80976-46-1
sodium salt of bicyclo<3.2.1>octa-2,6-dien-4-one p-toluenesulfonylhydrazone

: 81025-26-5
spiroocta-2',6'-diene>

: 81025-25-4
spiroocta-2',6'-diene>

: 81025-27-6
spiroocta-2',6'-diene>

: 80976-53-0
spiroocta-2',6'-diene>

Guidance literature:: In benzene; at 180 ℃; for 30h;
DOI:10.1021/ja00373a022

Reference yield:

: 80976-46-1
sodium salt of bicyclo<3.2.1>octa-2,6-dien-4-one p-toluenesulfonylhydrazone

: 81025-25-4
spiroocta-2',6'-diene>

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent Chromat_. / 200 °C / 5 Torr

2: benzene / 30 h / 180 °C

In benzene;
DOI:10.1021/ja00373a022