(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

Base Information

Chemical Name:(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester
CAS No.:104321-94-0
Molecular Formula:C₃₀H₄₂NO₇PS
Molecular Weight:591.706
Hs Code.:

(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

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Chemical Property of (Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

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Technology Process of (Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

There total 2 articles about (Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87360-02-9
N-(3,5-Dimethyl-phenyl)-N-((1S,2S,3R,4R)-3-hydroxy-4,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-benzenesulfonamide

: 104321-94-0
(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: C₆H₅N(CH₃)2

With N,N-dimethyl-aniline; 2: Michael-Arbuzov reaction;
DOI:10.1055/s-2003-45008

Reference yield:

: 104321-95-1
Chloro-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

: 122-52-1
triethyl phosphite

: 104321-94-0
(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

Guidance literature:: DOI:10.1055/s-2003-45008

Reference yield:

: 104321-94-0
(Diethoxy-phosphoryl)-acetic acid (1R,2R,3S,4S)-3-[benzenesulfonyl-(3,5-dimethyl-phenyl)-amino]-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl ester

: 676345-39-4
(1R,2R,3S,4S)-<3--2-bornyl>-(1S,5S)-5-vinyl-2-oxo-cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH

2.1: copper(I) cyanide; BF₃*Et₂O / diethyl ether / -80 °C

2.2: diethyl ether / 18 h / -80 - 20 °C

With boron trifluoride diethyl etherate; copper(l) cyanide; sodium hydride; In diethyl ether; 1.2: Wittig-Horner reaction;
DOI:10.1055/s-2003-45008