1,1'-bis(pentafluorophenyl)tetrahydrodigermane

Base Information

• Chemical Name: 1,1'-bis(pentafluorophenyl)tetrahydrodigermane
• CAS No.: 165334-33-8
• Molecular Formula: C₁₂H₄F₁₀Ge₂
• Molecular Weight: 483.328
• Mol file: 165334-33-8.mol

Synonyms:

Chemical Property of 1,1'-bis(pentafluorophenyl)tetrahydrodigermane

Chemical Property:

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Technology Process of 1,1'-bis(pentafluorophenyl)tetrahydrodigermane

There total 1 articles about 1,1'-bis(pentafluorophenyl)tetrahydrodigermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

(pentafluoro phenyl) germane (54008-41-2) → 1,1'-bis(pentafluorophenyl)tetrahydrodigermane (165334-33-8)

Guidance literature:

tris(triphenylphosphine)rhodium(l) chloride; In toluene; byproducts: H2; soln. of the Ge-compound was poured into a soln. of the catalyst, 20 h at 80°C; solvent evapd. in vacuo, residue extd. (hexane), hexane evapd. in vacuo, residue sublimed at 60°C (0.01 Torr); elem. anal.;

DOI:10.1007/BF00695834

upstream raw materials:

(pentafluoro phenyl) germane