[Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]

Base Information

Chemical Name:[Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]
CAS No.:85993-43-7
Molecular Formula:BF₄*C₁₇H₁₂FeNO₅
Molecular Weight:452.938
Hs Code.:

Synonyms:

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Chemical Property of [Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]

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Technology Process of [Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]

There total 1 articles about [Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 959609-36-0,88077-00-3,12093-05-9,1208904-82-8
cyclooctatetraeneiron tricarbonyl

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 85993-43-7,73141-35-2
[Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]

Guidance literature:: In acetone; byproducts: N2; to a stirred, cooled (-20°C) soln. of Fe-compd. (2.03 mmol) in acetone was added under N2 (N2C6H4NO2-p)(BF4) (2.03 mmol) in acetone;; after 40 min the red soln. was filtered and reduced in vol.; addn. of diethyl ether gave a ppt. which was recrystd. from acetone-diethyl ether;elem. anal.;;

Reference yield: 50.0%

: 85993-43-7,73141-35-2
[Fe(CO)3(η5-C8H8C6H4NO2-p)][BF4]

: 73130-68-4
[Fe(CO)3(η4-C8H7C6H4NO2-p)]

Guidance literature:: With pyridine; In acetone; to a stirred, cooled (-20°C) soln. of Fe-compd. (1.06 mmol) in acetone was added under N2 an excess of pyridine (3.8 mmol);; after warming to 30°C and stirring for 30 min the resulting red soln. was evapd. to dryness; the residue in Et2O was chromd. on alumina-hexane column; elution with hexane-diethyl ether; partial removal of thesolvent in vacuo; elem. anal.;;