bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF

Base Information

Chemical Name:bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF
CAS No.:82336-38-7
Molecular Formula:0C₃H₇NO*2C₂₄H₂₀P*0Mo₂S₁₀*0Mo₂S₁₂
Molecular Weight:1245.84
Hs Code.:

bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF

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Chemical Property of bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF

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Technology Process of bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF

There total 3 articles about bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: tetraphenylphosphonium tetrathiomolybdate

: 6493-73-8
dibenzyltrisulfide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 82336-38-7
bis (tetraphenylphosphonium) bis(μ-thio)[persulfidosulfidomolybdate(V)sulfidotetrasulfidomolybdate(V)]0.72 bis(μ-thio)[bis(sulfidotetrasulfidomolybdate(V))]0.28*0.5DMF

Guidance literature:: In N,N-dimethyl-formamide; under N2, (Ph4P)2MoS4 dissolved in DMF, to soln. added with stirring solid dibenzyl trisulfide, stirred for 5 min, added abs. ethanol, added diethyl ether, allowed to stand for 12 h; filtered, washed twice with abs. ethanol and three times with diethyl ether, dried, elem. anal.;