Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester

Base Information

• Chemical Name: Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester
• CAS No.: 103931-05-1
• Molecular Formula: C₅₉H₁₀₅N₂O₄PSi
• Molecular Weight: 965.553
• Mol file: 103931-05-1.mol

Synonyms:

Chemical Property of Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester

There total 5 articles about Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophenyl stearate (14617-86-8) → Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester (103931-05-1)

Guidance literature:

Multi-step reaction with 2 steps

2: triethylamine / CHCl₃ / 0.5 h / Ambient temperature

With triethylamine; In chloroform;

Reference yield:

C23H47Al (41765-25-7) → Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester (103931-05-1)

Guidance literature:

Multi-step reaction with 3 steps

1: hexane; diethyl ether / 0.5 h / Ambient temperature; addition of reagent - 15 deg C

3: triethylamine / CHCl₃ / 0.5 h / Ambient temperature

With triethylamine; In diethyl ether; hexane; chloroform;

Reference yield:

threo-4-(1-hydroxy-2-hexadecenyl)-2-phenyl-Δ2-oxazoline (78739-31-8,161968-12-3) → Diisopropyl-phosphoramidous acid (E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyl ester methyl ester (103931-05-1)

Guidance literature:

Multi-step reaction with 2 steps

2: triethylamine / CHCl₃ / 0.5 h / Ambient temperature

With triethylamine; In chloroform;

upstream raw materials:

N,N-diisopropylmethylphosphonamidic chloride

L-threo-3-0-(diphenyl-t-butylsylil)-2-N-stearoylsphingosine

4-nitrophenyl stearate

C₂₃H₄₇Al

Downstream raw materials:

Toluene-4-sulfonate(2-{[(E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyloxy]-methoxy-phosphanyloxy}-ethyl)-trimethyl-ammonium;

C₅₇H₁₀₁N₂O₆PSi

C₅₇H₁₀₁N₂O₅PSSi

Toluene-4-sulfonate(2-{[(E)-(2S,3S)-3-(tert-butyl-diphenyl-silanyloxy)-2-octadecanoylamino-octadec-4-enyloxy]-methoxy-phosphoryloxy}-ethyl)-trimethyl-ammonium;