N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

Base Information

Chemical Name:N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester
CAS No.:128747-59-1
Molecular Formula:C₄₆H₆₇N₅O₁₄
Molecular Weight:914.063
Hs Code.:

N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

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Chemical Property of N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

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Technology Process of N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

There total 5 articles about N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 30100-16-4
8-tert-butoxycarbonylaminooctanoic acid

: 57816-11-2,62928-83-0,75283-21-5,76498-06-1,76498-09-4
N-<2-O-(benzyl 2-acetamido-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

: 128747-59-1
N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(89)85019-0

Reference yield:

: 1002-57-9
8-Aminooctanoic acid

: 128747-59-1
N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / H₂O; dioxane / 12 h / Ambient temperature

2: 44 percent / DCC, DMAP / dimethylformamide / 3 h / Ambient temperature

With dmap; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85019-0

Reference yield:

: 41840-28-2
S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

: 128747-59-1
N-<2-O-(benzyl 2-acetamido-6-O-< 8-(tert-butoxycarbonylamino)octanoyl>-2,3-dideoxy-β-D-glucopyranosid-3-yl)-D-lactoyl>-L-alanyl-D-isoglutamine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / H₂O; dioxane / 12 h / Ambient temperature

2: 44 percent / DCC, DMAP / dimethylformamide / 3 h / Ambient temperature

With dmap; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(89)85019-0