[2,6-O(t)Bu₂C₆H₃]3GeOH

Base Information

Chemical Name:[2,6-O(t)Bu₂C₆H₃]3GeOH
CAS No.:1132827-18-9
Molecular Formula:C₄₂H₆₄GeO₇
Molecular Weight:753.556
Hs Code.:

[2,6-O(t)Bu<sub>2</sub>C<sub>6</sub>H<sub>3</sub>]3GeOH

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Chemical Property of [2,6-O(t)Bu₂C₆H₃]3GeOH

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Technology Process of [2,6-O(t)Bu₂C₆H₃]3GeOH

There total 2 articles about [2,6-O(t)Bu₂C₆H₃]3GeOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.6%

: 428441-32-1
silver tetrakis([2,2,2-trifluoro-1,1-bis(trifluoromethyl)ethyl]oxy)aluminate

: 869500-35-6
Ge(Br)[2,6-di-tert-butoxyphenyl)3

: 1132827-18-9
[2,6-O(t)Bu₂C₆H₃]3GeOH

: [2,6-O(t)Bu₂C₆H₃]3GeO(t)Bu

Guidance literature:: With KO(t)Bu; In tetrahydrofuran; dichloromethane; byproducts: AgBr, KAl[OC(CF3)3]4, iso-butene; under N2 (vac.); Ge- and AgAl-contg. compds. were added to a flask in a glove box; cooling to -78°C and -78°C cold CH2Cl2 was added; soln. was warmed to -30°C and stirred for 2 d; a soln. of KO(t)Bu in THF was added at -40°C; the solvent was removed and the residue extd. with toluene; this soln. was concd.;
DOI:10.1039/b818931e

Reference yield:

: 869500-36-7
[Li(μ-2,6-di-tert-butoxyphenyl)]3

: 1132827-18-9
[2,6-O(t)Bu₂C₆H₃]3GeOH

: [2,6-O(t)Bu₂C₆H₃]3GeO(t)Bu

Guidance literature:: Multi-step reaction with 2 steps

1: not given

2: KO(t)Bu / dichloromethane; tetrahydrofuran

With KO(t)Bu; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b818931e