(3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

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Chemical Name:(3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;
CAS No.:111614-51-8
Molecular Formula:C₁₆H₃₆N*C₁₇H₁₆N₅O₆S₂
Molecular Weight:692.944
Hs Code.:

Synonyms:

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Chemical Property of (3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

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Technology Process of (3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

There total 3 articles about (3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78905-28-9,81767-89-7
cis-3-azido-2-oxo-4-(2-phenylethenyl)-1-azetidine

: 111614-51-8
(3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine-sulfur trioxide complex / 1.) pyridine, 80 deg C, 2 h; 2.) CH₂Cl₂

2: tetrahydrofuran; dimethylformamide / 1 h / Ambient temperature

3: 500 mg / tetrahydrofuran; dimethylformamide / 8 h / 50 °C

With sulfur trioxide pyridine complex; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1139/v87-014

Reference yield:

: (3S,4R)-3-Azido-1-[bis-(4-methoxy-phenyl)-methyl]-4-((E)-styryl)-azetidin-2-one

: 111614-51-8
(3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 0.75 h / -5 - 0 °C

2: 1.) pyridine-sulfur trioxide complex / 1.) pyridine, 80 deg C, 2 h; 2.) CH₂Cl₂

3: tetrahydrofuran; dimethylformamide / 1 h / Ambient temperature

4: 500 mg / tetrahydrofuran; dimethylformamide / 8 h / 50 °C

With ammonium cerium(IV) nitrate; sulfur trioxide pyridine complex; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1139/v87-014

Reference yield:

: 4-styryl-3-azido-2-oxo-1-azetidine sulfonic acid tetrabutylammonium salt

: 111614-51-8
(3S,4R)-3-{2-(2-Amino-thiazol-4-yl)-2-[(Z)-methoxyimino]-acetylamino}-2-oxo-4-((E)-styryl)-azetidine-1-sulfonatetetrabutyl-ammonium;

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; dimethylformamide / 1 h / Ambient temperature

2: 500 mg / tetrahydrofuran; dimethylformamide / 8 h / 50 °C

In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1139/v87-014