C₄₂H₄₅NO₃

Base Information

Chemical Name:C₄₂H₄₅NO₃
CAS No.:1246452-36-7
Molecular Formula:C₄₂H₄₅NO₃
Molecular Weight:611.824
Hs Code.:

C<sub>42</sub>H<sub>45</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₄₂H₄₅NO₃

Chemical Property:

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Technology Process of C₄₂H₄₅NO₃

There total 5 articles about C₄₂H₄₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246452-34-5
C₁₄H₁₉I₂NO₃

: 1246452-36-7
C₄₂H₄₅NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 50 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; In tetrahydrofuran; 1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242

Reference yield:

: 49617-79-0
1,3-diiodo-5-methylbenzene

: 1246452-36-7
C₄₂H₄₅NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 70 °C

2.1: hydrazine hydrate / ethanol / Reflux

2.2: 20 °C

2.3: 20 °C

3.1: triethylamine / N,N-dimethyl-formamide / 20 °C

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 50 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 1.1: Williamson synthesis / 4.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242

Reference yield:

: 1246452-32-3
N-[3-(3,5-diiodophenoxy)propyl]phthalimide

: 1246452-36-7
C₄₂H₄₅NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / ethanol / Reflux

1.2: 20 °C

1.3: 20 °C

2.1: triethylamine / N,N-dimethyl-formamide / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 18 h / 50 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; 3.1: Sonogashira-Hagihara coupling;
DOI:10.1021/ma1016242