allylbenzene chromiumtricarbonyl

Base Information

Chemical Name:allylbenzene chromiumtricarbonyl
CAS No.:57003-19-7
Molecular Formula:C₁₂H₁₀CrO₃
Molecular Weight:254.206
Hs Code.:

Synonyms:

Suppliers and Price of allylbenzene chromiumtricarbonyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allylbenzene chromiumtricarbonyl

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Technology Process of allylbenzene chromiumtricarbonyl

There total 2 articles about allylbenzene chromiumtricarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 138678-62-3,138678-76-9
(CO)3Cr(C₆H₅CH(CHCH₂)CH(OH)C₆H₅)

: 865-47-4
potassium tert-butylate

: 72924-51-7,98169-43-8
tricarbonyl(1-phenylpropene)chromium(O)

: 57003-19-7
allylbenzene chromiumtricarbonyl

: (η6-1,4-diphenyl-1,3-butadiene)tricarbonylchromium(0)

Guidance literature:: In tetrahydrofuran; under N2, stirred for 20 min at 20°C; hydrolysed, extd. (ether), dried (MgSO4), solvent evapd., chromy. (silica gel, ether/petroleum ether); yield of allyl- and propenylbenzene tricarbonyl: 30%;
DOI:10.1016/0022-328X(91)80262-I

Reference yield: 2.5%

: (CO)3Cr(C₆H₅CHCHCH₂CH(OH)C₆H₅)

: 865-47-4
potassium tert-butylate

: 72924-51-7,98169-43-8
tricarbonyl(1-phenylpropene)chromium(O)

: 57003-19-7
allylbenzene chromiumtricarbonyl

: (η6-1,4-diphenyl-1,3-butadiene)tricarbonylchromium(0)

Guidance literature:: In tetrahydrofuran; under N2, stirred for 20 min; hydrolysed, extd. (ether), dried (MgSO4), solvent evapd., chromy. (silica gel, ether/petroleum ether); yield of allyl- and propenylbenzene tricarbonyl: 8.5%;
DOI:10.1016/0022-328X(91)80262-I

Reference yield: 74.0%

: 57003-19-7
allylbenzene chromiumtricarbonyl

: 2155-96-6
Diphenylvinylphosphine

: 1351283-69-6
(η**(6)-allylbenzene)(diphenylvinylphosphine)chromium(0) dicarbonyl

Guidance literature:: In benzene; Irradiation (UV/VIS); standard Schlenk technique; Cr complex and phosphine deriv. dissoloved in benzene under Ar; irradiated with Hg lamp; stirred for 7 h at room temp.; filtered, concd. under reduced pressure; residue purified by silica gel chromy.; elem. anal.;
DOI:10.1016/j.jorganchem.2011.05.006