{Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)}

Base Information

Chemical Name:{Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)}
CAS No.:151007-75-9
Molecular Formula:C₄₂H₄₆NiO₆P₂S₂
Molecular Weight:831.593
Hs Code.:

{Ni(S<sub>2</sub>C<sub>6</sub>H<sub>2</sub>(O<sub>6</sub>C<sub>10</sub>H<sub>20</sub>))((P(C<sub>6</sub>H<sub>5</sub>)2)2C<sub>2</sub>H<sub>4</sub>)}

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Chemical Property of {Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)}

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Technology Process of {Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)}

There total 1 articles about {Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 14647-23-5
cis-[NiCl₂(1,2-bis(diphenylphosphino)ethane)]

: 150921-10-1
2,3,5,6,8,9,11,12,14,15-Decahydro-1,4,7,10,13,16-benzohexaoxacyclooctadecine-18,19-dithiol

: 151007-75-9
{Ni(S₂C₆H₂(O₆C₁₀H₂₀))((P(C₆H₅)2)2C₂H₄)}

Guidance literature:: With potassium; In methanol; dichloromethane; under N2: treating of 1.50 mmol crown ether benzodithiolene with 3.1 mmol K-metal in CH3OH; addn. of 1.48 mmol (Ni((P(C6H5)2)2C2H4)Cl2) in CH2Cl2; stirring for 4 h at room temperature; pptn.; stirring overnight; filtration;; pumping to dryness; washing with acetone; dissolving in CHCl3; evapn. to dryness; chromy. (silica gel, CH2Cl2/CH3OH (10:1)); not pure;;