Technology Process of C39H51N3O7
There total 9 articles about C39H51N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydroxide / water
1.3: 215 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide
3.1: ammonium acetate
4.1: lithium aluminium tetrahydride
5.1: dmap
6.1: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); ammonium acetate; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate;
In
water; N,N-dimethyl-formamide;
3.1: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate
2.1: sodium methylate / methanol
2.2: 160 °C
3.1: sodium hydroxide / water
3.3: 215 °C
4.1: trichlorophosphate / N,N-dimethyl-formamide
5.1: ammonium acetate
6.1: lithium aluminium tetrahydride
7.1: dmap
8.1: tetrakis(triphenylphosphine) palladium(0); copper(l) chloride; lithium chloride
With
dmap; lithium aluminium tetrahydride; tetrakis(triphenylphosphine) palladium(0); ammonium acetate; sodium methylate; potassium carbonate; copper(l) chloride; lithium chloride; sodium hydroxide; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
2.1: Hemetsberger indole cyclization / 5.1: Henry reaction;
DOI:10.1002/chem.201103605
