OW(C₆H₅C₂H)(S₂CN(CH₃)2)2

Base Information

• Chemical Name: OW(C₆H₅C₂H)(S₂CN(CH₃)2)2
• CAS No.: 76429-50-0
• Molecular Formula: C₁₄H₁₈N₂OS₄W
• Molecular Weight: 542.424
• Mol file: 76429-50-0.mol

Synonyms:

Chemical Property of OW(C₆H₅C₂H)(S₂CN(CH₃)2)2

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of OW(C₆H₅C₂H)(S₂CN(CH₃)2)2

There total 1 articles about OW(C₆H₅C₂H)(S₂CN(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

carbonyl(η2-phenylacetylene)bis(N,N-dimethyldithiocarbamato)tungsten(II) (98735-60-5) + Mo2O3(4+)*4S2P(OC2H5)2(1-)=Mo2O3(S2P(OC2H5)2)4 (27862-11-9) → OW(C6H5C2H)(S2CN(CH3)2)2 (76429-50-0) + OMo(2+)*2S2P(OC2H5)2(1-)=OMo(S2P(OC2H5)2)2

Guidance literature:

In dichloromethane; byproducts: CO; under inert atmosphere, equimolar amt. of Mo- and W-complexes dissolvedin CH2Cl2, stirred at room temp. for 4 h; filtered, filtrate evapd. to dryness under vac., treated with Et2O, filtered, washed with Et2O, dried in vac.; elem. anal.;

DOI:10.1021/ic50218a056

upstream raw materials:

carbonyl(η2-phenylacetylene)bis(N,N-dimethyldithiocarbamato)tungsten(II)

Mo₂O₃⁽⁴⁺⁾*4S₂P(OC₂H₅)2^(1-)=Mo₂O₃(S₂P(OC₂H₅)2)4