Technology Process of C35H37N3O5
There total 5 articles about C35H37N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
2: toluene-4-sulfonic acid / ethyl acetate; ethanol / 2 h / 0 - 20 °C
3: triethylamine / dichloromethane / 3 h / 4 - 20 °C
4: sodium tris(acetoxy)borohydride; acetic acid / 16 h / 20 °C
With
sodium tris(acetoxy)borohydride; caesium carbonate; toluene-4-sulfonic acid; acetic acid; triethylamine;
In
ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400823w
- Guidance literature:
-
Multi-step reaction with 4 steps
1: caesium carbonate / N,N-dimethyl-formamide / 20 °C
2: toluene-4-sulfonic acid / ethyl acetate; ethanol / 2 h / 0 - 20 °C
3: triethylamine / dichloromethane / 3 h / 4 - 20 °C
4: sodium tris(acetoxy)borohydride; acetic acid / 16 h / 20 °C
With
sodium tris(acetoxy)borohydride; caesium carbonate; toluene-4-sulfonic acid; acetic acid; triethylamine;
In
ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm400823w
- Guidance literature:
-
With
sodium tris(acetoxy)borohydride; acetic acid;
at 20 ℃;
for 16h;
DOI:10.1021/jm400823w