N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide

Base Information

• Chemical Name: N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide
• CAS No.: 114676-02-7
• Molecular Formula: C₃₂H₁₇N₃O₂
• Molecular Weight: 475.506
• Mol file: 114676-02-7.mol

Synonyms:

Chemical Property of N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide

There total 5 articles about N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-naphtho[1,2,3,4-def]chrysen-8-yl-4-phenyl-[1,2,4]triazolidine-3,5-dione (55425-09-7) → N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide (114676-02-7)

Guidance literature:

With pyridine; bromine; In dichloromethane; at 8 ℃; for 96h;

Reference yield:

Dibenzo[a,e]pyrene (192-65-4) + 1-naphtho[1,2,3,4-def]chrysen-8-yl-4-phenyl-[1,2,4]triazolidine-3,5-dione (55425-09-7) → N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide (114676-02-7) + 1,2-bis(8-naphtho<1,2,3,4-def>chrysenyl)-4-phenyl-1,2,4-triazolidine-3,5-dione

Guidance literature:

With pyridine; bromine; In dichloromethane; at 8 ℃; for 144h;

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → N-Phenylbenzochryseno<4,5,6-ghij>phthalazine-5,6-dicarboximide (114676-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 21 percent Turnov_. / CH₂Cl₂ / 44 h / Ambient temperature

2: 0.4 mg / Br₂, pyridine / CH₂Cl₂ / 144 h / 8 °C

With pyridine; bromine; In dichloromethane;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

Dibenzo[a,e]pyrene

1-naphtho[1,2,3,4-def]chrysen-8-yl-4-phenyl-[1,2,4]triazolidine-3,5-dione