(S)-(+)-fluoromevalonolactone

Base Information

Chemical Name:(S)-(+)-fluoromevalonolactone
CAS No.:119066-08-9
Molecular Formula:C₆H₉FO₃
Molecular Weight:148.134
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(+)-fluoromevalonolactone

Chemical Property:

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Technology Process of (S)-(+)-fluoromevalonolactone

There total 7 articles about (S)-(+)-fluoromevalonolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 118965-27-8
methyl 3-acetoxy-3-fluoromethyl-5-hydroxypentanoate

: 119066-08-9,2822-77-7
(S)-(+)-fluoromevalonolactone

Guidance literature:: With potassium hydroxide; In methanol; Ambient temperature;

Reference yield:

: 2267-53-0
4-fluoromethyl-1,6-heptadien-4-ol

: 119066-08-9,2822-77-7
(S)-(+)-fluoromevalonolactone

Guidance literature:: Multi-step reaction with 7 steps

1: ozone / ethyl acetate / 5 h / -70 °C

2: 30 percent H₂O₂, glacial acetic acid, conc. H₂SO₄ / H₂O / 4 h / Heating

3: conc. H₂SO₄ / 10 h / Heating

4: 95 percent / PLE (Sigma) / 10 h / 25 °C / pH = 8

5: 98 percent / 4-dimethylaminopyridine / Ambient temperature

6: 22 percent / borane-dimethyl sulfide / tetrahydrofuran / 8 h / Ambient temperature

7: 58 percent / 0.1 N aq. KOH / methanol / Ambient temperature

With dmap; potassium hydroxide; dimethylsulfide borane complex; PLE (Sigma); sulfuric acid; dihydrogen peroxide; ozone; acetic acid; In tetrahydrofuran; methanol; water; ethyl acetate;

Reference yield:

: 682-14-4
3-Hydroxy-3-fluormethyl-glutarsaeure

: 119066-08-9,2822-77-7
(S)-(+)-fluoromevalonolactone

Guidance literature:: Multi-step reaction with 5 steps

1: conc. H₂SO₄ / 10 h / Heating

2: 95 percent / PLE (Sigma) / 10 h / 25 °C / pH = 8

3: 98 percent / 4-dimethylaminopyridine / Ambient temperature

4: 22 percent / borane-dimethyl sulfide / tetrahydrofuran / 8 h / Ambient temperature

5: 58 percent / 0.1 N aq. KOH / methanol / Ambient temperature

With dmap; potassium hydroxide; dimethylsulfide borane complex; PLE (Sigma); sulfuric acid; In tetrahydrofuran; methanol;