Technology Process of C35H41NO4
There total 6 articles about C35H41NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at -78 ℃;
for 0.5h;
regioselective reaction;
Inert atmosphere;
Cooling with acetone-dry ice;
DOI:10.1021/ja5013323
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 7 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 60 °C / Inert atmosphere
2.1: triethylamine; dmap / tetrahydrofuran / 1 h / Inert atmosphere
3.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice
With
dmap; boron trifluoride diethyl etherate; triethylamine; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; dichloromethane;
1.2: |Suzuki Coupling;
DOI:10.1021/ja5013323
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; dmap / tetrahydrofuran / 1 h / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -78 °C / Inert atmosphere; Cooling with acetone-dry ice
With
dmap; boron trifluoride diethyl etherate; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja5013323
