OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)

Base Information

Chemical Name:OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)
CAS No.:258328-65-3
Molecular Formula:C₄₇H₃₈BrN₄OOsP₂
Molecular Weight:1006.9
Hs Code.:

OsBrCO(P(C<sub>6</sub>H<sub>5</sub>)3)2(NC<sub>5</sub>H<sub>4</sub>N<sub>2</sub>C<sub>5</sub>H<sub>4</sub>N)

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Chemical Property of OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)

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Technology Process of OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)

There total 1 articles about OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2633-03-6
2,2'-azopyridine

: 606142-02-3,16971-32-7
mer-Os(PPh3)3HBr(CO)

: 258328-65-3
OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)

Guidance literature:: In n-heptane; to excess of ligand dissolved in heptane was added Os-complex, mixt. was heated to reflux for 2 h under N2; mixt. was cooled, filtered, dissolved in benzene, recovered by evapn. under reduced pressure, washed with MeCN and hexane, dried in vacuo; elem. anal.;
DOI:10.1021/ic9908322

Reference yield: 80.0%

: ammonium hexafluorophosphate

: 258328-65-3
OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)

: 258328-69-7
OsBrCO(P(C₆H₅)3)2(NC₅H₄N₂C₅H₄N)⁽¹⁺⁾*PF₆^(1-)=OsBrCO(C₅H₄NN₂C₅H₄N)(P(C₆H₅)3)2PF₆

Guidance literature:: In dichloromethane; acetonitrile; to soln. of Os-complex in CH2Cl2 was added MeCN soln. of NH4PF6, mixt. was stirred in air; solvent was removed under reduced pressure, solid was washed with water, dried in vacuo, CH2Cl2 soln. was chromd. on silica gel column with MeCN-benzene; elem. anal.;
DOI:10.1021/ic9908322