4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

Base Information

Chemical Name:4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}
CAS No.:124652-51-3
Molecular Formula:C₂₈H₄₆B₂N₄Sn
Molecular Weight:579.032
Hs Code.:

Synonyms:

Suppliers and Price of 4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

There total 1 articles about 4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10375-18-5
Bis-tert.-butylamino-phenylboran

: 124652-51-3
4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

Guidance literature:: Multi-step reaction with 2 steps

1: n-C₄H₉Li / hexane

2: hexane

With n-C₄H₉Li; In hexane;

Reference yield:

: 7791-25-5
sulfuryl dichloride

: 124652-51-3
4,4'-spirobis{1,3-di(tert-butyl)-2-phenyl-1,3-diaza-2-bora-4-tinacyclobutane}

: Sn[PhB(μ-N-t-Bu)2]2Cl

Guidance literature:: In diethyl ether; byproducts: LiCl; (N2, Schlenk) a soln. of SO2Cl2 in diethyl ether was added to a soln. ofcomplex in diethyl ether at -80°C, the mixt. was allowed to warm up to ca. -40°C; not isolated, detected by ESR-spectra;
DOI:10.1139/V08-183