C₂₆H₂₃ClN₂O₂

Base Information

Chemical Name:C₂₆H₂₃ClN₂O₂
CAS No.:1616558-03-2
Molecular Formula:C₂₆H₂₃ClN₂O₂
Molecular Weight:430.934
Hs Code.:

C<sub>26</sub>H<sub>23</sub>ClN<sub>2</sub>O<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₃ClN₂O₂

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Technology Process of C₂₆H₂₃ClN₂O₂

There total 5 articles about C₂₆H₂₃ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1627704-44-2
C₃₀H₃₁ClN₂O₂

: 1616558-03-2
C₂₆H₂₃ClN₂O₂

Guidance literature:: With trifluoroacetic acid;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 59247-47-1
tert-butyl-4-bromobenzoate

: 1616558-03-2
C₂₆H₂₃ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tert-butyl XPhos / N,N-dimethyl-formamide / 90 °C

2: lithium hexamethyldisilazane; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / -78 °C

3: sodium carbonate / toluene / Reflux

4: trifluoroacetic acid

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N,N,N,N,-tetramethylethylenediamine; sodium carbonate; caesium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane; tert-butyl XPhos; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2014.05.036

Reference yield:

: 1616558-02-1
C₁₇H₂₂N₂O₂

: 1616558-03-2
C₂₆H₂₃ClN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hexamethyldisilazane; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / -78 °C

2: sodium carbonate / toluene / Reflux

3: trifluoroacetic acid

With N,N,N,N,-tetramethylethylenediamine; sodium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmcl.2014.05.036