C₂₂H₃₁F₃INO₅Si

Base Information

Chemical Name:C₂₂H₃₁F₃INO₅Si
CAS No.:1315503-95-7
Molecular Formula:C₂₂H₃₁F₃INO₅Si
Molecular Weight:601.477
Hs Code.:

C<sub>22</sub>H<sub>31</sub>F<sub>3</sub>INO<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₁F₃INO₅Si

Chemical Property:

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Technology Process of C₂₂H₃₁F₃INO₅Si

There total 2 articles about C₂₂H₃₁F₃INO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338441-04-5
C₁₄H₂₇IO₅Si

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 1315503-95-7
C₂₂H₃₁F₃INO₅Si

Guidance literature:: With caesium carbonate; In dichloromethane; at 20 ℃; for 3.5h;
DOI:10.1021/ja205339p

Reference yield:

: 1,4-di-O-acetyl-3-O-(tert-butyldimethyl)silyl-2,6-dideoxy-2-iodo-Dglucopyranoside

: 1315503-95-7
C₂₂H₃₁F₃INO₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C

2: caesium carbonate / dichloromethane / 3.5 h / 20 °C

With caesium carbonate; hydrazine hydrate; In methanol; dichloromethane;
DOI:10.1021/ja205339p

Reference yield:

: 1315503-95-7
C₂₂H₃₁F₃INO₅Si

: 1315504-00-7
C₃₂H₄₀F₃I₂NO₁₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / -78 - 20 °C / Molecular sieve

1.2: 0.5 h / -78 °C

2.1: triethylamine tris(hydrogen fluoride) / acetonitrile / 20 - 60 °C

3.1: dichloromethane / -50 - 20 °C / Molecular sieve

3.2: 0.5 h / -78 °C

4.1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C

5.1: caesium carbonate / dichloromethane / 3.5 h / 20 °C

With caesium carbonate; hydrazine hydrate; triethylamine tris(hydrogen fluoride); In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja205339p