(1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

Base Information

Chemical Name:(1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol
CAS No.:69100-21-6
Molecular Formula:C₁₁H₁₉NO
Molecular Weight:181.278
Hs Code.:

Synonyms:

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Chemical Property of (1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

Chemical Property:

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Technology Process of (1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

There total 7 articles about (1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 71610-20-3,71630-04-1
(1aα,3aα,5β,7aα,7bα)-N-(decahydronaphth<1,2-b>oxiren-5-yl)-2,2,2-trifluoro-N-methylacetamide

: 69100-21-6
(1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

Guidance literature:: With potassium carbonate; In methanol; water; for 2h; Heating;
DOI:10.1021/jo00155a014

Reference yield:

: 21110-68-9
2-ethenylbicyclo<2.2.2>oct-5-en-2-ol

: 69100-21-6
(1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / KH / 18-crown-6 / 1,2-dimethoxy-ethane / 14 h / Ambient temperature

2: 92 percent / sodium cyanoborohydride / methanol / 24 h / Ambient temperature

3: 56 percent / NaCO₃ / diethyl ether; tetrahydrofuran / 1.) ice bath, 2.) ice bath remove, 30 min.

4: 70 percent / m-chloroperbenzoic acid, NaHCO₃ / CH₂Cl₂ / 15 h / Ambient temperature

5: 91 percent / K₂CO₃ / methanol; H₂O / 2 h / Heating

With potassium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; 18-crown-6 ether; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water;
DOI:10.1021/jo00155a014

Reference yield:

: 936-37-8
cis-3,4,4a,7,8,8a-hexahydro-2(1H)-naphthalenone

: 69100-21-6
(1α,2β,4aβ,6α,8aβ)-decahydro-9-methylnaphthalen-1,6-imin-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / sodium cyanoborohydride / methanol / 24 h / Ambient temperature

2: 56 percent / NaCO₃ / diethyl ether; tetrahydrofuran / 1.) ice bath, 2.) ice bath remove, 30 min.

3: 70 percent / m-chloroperbenzoic acid, NaHCO₃ / CH₂Cl₂ / 15 h / Ambient temperature

4: 91 percent / K₂CO₃ / methanol; H₂O / 2 h / Heating

With sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/jo00155a014