3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one

Base Information

Chemical Name:3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one
CAS No.:121851-35-2
Molecular Formula:C₁₆H₁₈OS
Molecular Weight:258.384
Hs Code.:
DSSTox Substance ID:DTXSID10557974
Nikkaji Number:J464.895A
Wikidata:Q82440063
Mol file:121851-35-2.mol

Synonyms:121851-35-2;DTXSID10557974;3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one

Suppliers and Price of 3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:258.10783637
Heavy Atom Count:18
Complexity:337

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCC1=C(C(=O)CCC1)SC2=CC=CC=C2

Technology Process of 3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one

There total 4 articles about 3-(But-3-en-1-yl)-2-(phenylsulfanyl)cyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 121851-35-2
3-(3-Butenyl)-2-(phenylthio)-2-cyclohexen-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) THF, reflux, 2) THF, 1.5 h, r.t.

2: 86 percent / 30percent H₂O₂, 6N NaOH / methanol / 1 h / Ambient temperature

3: 1) KH / 1) THF, 5 min, 2) THF, 24 h, r.t.

With sodium hydroxide; dihydrogen peroxide; potassium hydride; magnesium; In methanol;
DOI:10.1021/jo00030a022

Reference yield:

: 22627-45-8
3-(3-butenyl)cyclohex-2-en-1-one

: 121851-35-2
3-(3-Butenyl)-2-(phenylthio)-2-cyclohexen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 30percent H₂O₂, 6N NaOH / methanol / 1 h / Ambient temperature

2: 1) KH / 1) THF, 5 min, 2) THF, 24 h, r.t.

With sodium hydroxide; dihydrogen peroxide; potassium hydride; In methanol;
DOI:10.1021/jo00030a022