N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Base Information

Chemical Name:N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine
CAS No.:1154745-04-6
Molecular Formula:C₆₅H₇₉BrN₄O₄
Molecular Weight:1060.27
Hs Code.:

N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Chemical Property of N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

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Technology Process of N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

There total 1 articles about N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇₅H₉₅BrN₄O₈

: 1154745-04-6
N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tetasy.2009.01.017

Reference yield: 81.0%

: 1154745-04-6
N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: 1155930-47-4,1155926-80-9,1155930-50-9
(+/-)-2,8,14-tribenzyl-5,11,17,23-tetra-tert-butyl-25,26,27,28-tetramethoxy-2,8,14,2'-tetraazacalix[4]arene

Guidance literature:: N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 0.0833333h; Reflux;

With sodium t-butanolate; In toluene; for 6h; Reflux;
DOI:10.1016/j.tetasy.2009.01.017

Reference yield:

: 1154745-04-6
N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine

: (-)-2,8,14-tribenzyl-5,11,17,23-tetra-tert-butyl-25,26,27,28-tetramethoxy-2,8,14,2'-tetraazacalix[4]arene

Guidance literature:: N-benzyl-N-{3-[N-benzyl-3-(N-benzyl-3-bromo-5-tertbutyl-2-methoxyanilino)-5-tert-butyl-2-methoxyanilino]-5-tert-butyl-2-methoxyphenyl}-5-tert-butyl-2-methoxy-1,3-phenylenediamine; With (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; for 0.0833333h; Reflux;

With sodium t-butanolate; In toluene; for 6h; optical yield given as %ee; Reflux;
DOI:10.1016/j.tetasy.2009.01.017