C₅₀H₇₃N₃O₂₂

Base Information

• Chemical Name: C₅₀H₇₃N₃O₂₂
• CAS No.: 1251911-85-9
• Molecular Formula: C₅₀H₇₃N₃O₂₂
• Molecular Weight: 1068.14
• Mol file: 1251911-85-9.mol

Synonyms:

Chemical Property of C₅₀H₇₃N₃O₂₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₇₃N₃O₂₂

There total 4 articles about C₅₀H₇₃N₃O₂₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tert-butyloxycarbonyl-Nε-benzyloxycarbonyl-L-lysinyl-octylamide (138277-52-8) → C50H73N3O22 (1251911-85-9)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 6 h / 0 °C

2: triethylamine / ethyl methyl ether / 24 h / 65 °C / Inert atmosphere

3: pyridine / 12 h / 0 °C

With pyridine; triethylamine; trifluoroacetic acid; In ethyl methyl ether; dichloromethane;

DOI:10.1039/c0nj00024h

Reference yield:

benzyl N-[(5S)-5-amino-6-(octylamino)-6-oxo-hexyl]carbamate (136994-44-0) → C50H73N3O22 (1251911-85-9)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / ethyl methyl ether / 24 h / 65 °C / Inert atmosphere

2: pyridine / 12 h / 0 °C

With pyridine; triethylamine; In ethyl methyl ether;

DOI:10.1039/c0nj00024h

Reference yield:

n-Octylamine (111-86-4) → C50H73N3O22 (1251911-85-9)

Guidance literature:

Multi-step reaction with 4 steps

1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 6 h / 0 °C

3: triethylamine / ethyl methyl ether / 24 h / 65 °C / Inert atmosphere

4: pyridine / 12 h / 0 °C

With pyridine; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In ethyl methyl ether; dichloromethane;

DOI:10.1039/c0nj00024h

upstream raw materials:

N-tert-butyloxycarbonyl-N^ε-benzyloxycarbonyl-L-lysinyl-octylamide

benzyl N-[(5S)-5-amino-6-(octylamino)-6-oxo-hexyl]carbamate

n-Octylamine

Boc-Lys(Z)-OH