C₆₀H₈₅NO₁₀

Base Information

Chemical Name:C₆₀H₈₅NO₁₀
CAS No.:202462-25-7
Molecular Formula:C₆₀H₈₅NO₁₀
Molecular Weight:980.336
Hs Code.:

C<sub>60</sub>H<sub>85</sub>NO<sub>10</sub>

Synonyms:

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Chemical Property of C₆₀H₈₅NO₁₀

Chemical Property:

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Technology Process of C₆₀H₈₅NO₁₀

There total 14 articles about C₆₀H₈₅NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33628-52-3
3α,7α-diacetoxy-24-phenyl-5β-cholan-24-oic acid

: 202462-25-7
C₆₀H₈₅NO₁₀

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) Pb(OAc)4, 2.) I₂ / 1.) CCl₄, irradiation, reflux, 20 min, 2.) CCl₄, reflux, 70 min

2: 90 percent / DMSO, 2,4,6-collidine / 1.5 h / 150 °C

3: 1.) NaN(SiMe₃)2 / 1.) THF, RT, 30 min, 2.) THF, 0 deg C, 1 h

4: 92 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

5: dimethylformamide / 17 h / Ambient temperature

6: H₂ / Pd(OH)2/C / ethanol / 96 h

7: 95 percent / pyridine / CH₂Cl₂ / 4 h / 0 °C

8: 1.) 2,6-di-tert-butyl-4-methylpyridine, triflic anhydride / 1.) CH₂Cl₂, -78 deg C, 5 min, 2.) CH₂Cl₂, from -78 deg C to -20 deg C

9: 96 percent / 46percent aq. HF / acetonitrile / 3.5 h / Ambient temperature

10: 95 percent / pyridinium dichromate, molecular sieves 4A / CH₂Cl₂ / 4.7 h / Ambient temperature

11: 96 percent / camphorsulfonic acid / CH₂Cl₂; methanol / 2 h / Ambient temperature

12: LiAlH₄ / tetrahydrofuran / 6 h / Ambient temperature

13: DMAP, pyridine / 4 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; lead(IV) acetate; dmap; lithium aluminium tetrahydride; dipyridinium dichromate; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen fluoride; hydrogen; iodine; sodium hexamethyldisilazane; dimethyl sulfoxide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0968-0896(97)00170-3

Reference yield:

: 474-25-9
chenodeoxycholic acid

: 202462-25-7
C₆₀H₈₅NO₁₀

Guidance literature:: Multi-step reaction with 14 steps

1: 88 percent / 4-dimethylaminopyridine, pyridine / 4 h / Ambient temperature

2: 1.) Pb(OAc)4, 2.) I₂ / 1.) CCl₄, irradiation, reflux, 20 min, 2.) CCl₄, reflux, 70 min

3: 90 percent / DMSO, 2,4,6-collidine / 1.5 h / 150 °C

4: 1.) NaN(SiMe₃)2 / 1.) THF, RT, 30 min, 2.) THF, 0 deg C, 1 h

5: 92 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

6: dimethylformamide / 17 h / Ambient temperature

7: H₂ / Pd(OH)2/C / ethanol / 96 h

8: 95 percent / pyridine / CH₂Cl₂ / 4 h / 0 °C

9: 1.) 2,6-di-tert-butyl-4-methylpyridine, triflic anhydride / 1.) CH₂Cl₂, -78 deg C, 5 min, 2.) CH₂Cl₂, from -78 deg C to -20 deg C

10: 96 percent / 46percent aq. HF / acetonitrile / 3.5 h / Ambient temperature

11: 95 percent / pyridinium dichromate, molecular sieves 4A / CH₂Cl₂ / 4.7 h / Ambient temperature

12: 96 percent / camphorsulfonic acid / CH₂Cl₂; methanol / 2 h / Ambient temperature

13: LiAlH₄ / tetrahydrofuran / 6 h / Ambient temperature

14: DMAP, pyridine / 4 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; lead(IV) acetate; dmap; lithium aluminium tetrahydride; dipyridinium dichromate; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen fluoride; hydrogen; iodine; sodium hexamethyldisilazane; dimethyl sulfoxide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0968-0896(97)00170-3

Reference yield:

: 168417-79-6
23-iodo-24-nor-5β-cholane-3α,7α-diyl diacetate

: 202462-25-7
C₆₀H₈₅NO₁₀

Guidance literature:: Multi-step reaction with 12 steps

1: 90 percent / DMSO, 2,4,6-collidine / 1.5 h / 150 °C

2: 1.) NaN(SiMe₃)2 / 1.) THF, RT, 30 min, 2.) THF, 0 deg C, 1 h

3: 92 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

4: dimethylformamide / 17 h / Ambient temperature

5: H₂ / Pd(OH)2/C / ethanol / 96 h

6: 95 percent / pyridine / CH₂Cl₂ / 4 h / 0 °C

7: 1.) 2,6-di-tert-butyl-4-methylpyridine, triflic anhydride / 1.) CH₂Cl₂, -78 deg C, 5 min, 2.) CH₂Cl₂, from -78 deg C to -20 deg C

8: 96 percent / 46percent aq. HF / acetonitrile / 3.5 h / Ambient temperature

9: 95 percent / pyridinium dichromate, molecular sieves 4A / CH₂Cl₂ / 4.7 h / Ambient temperature

10: 96 percent / camphorsulfonic acid / CH₂Cl₂; methanol / 2 h / Ambient temperature

11: LiAlH₄ / tetrahydrofuran / 6 h / Ambient temperature

12: DMAP, pyridine / 4 h / Ambient temperature

With pyridine; 2,4,6-trimethyl-pyridine; dmap; lithium aluminium tetrahydride; dipyridinium dichromate; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen fluoride; hydrogen; sodium hexamethyldisilazane; dimethyl sulfoxide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0968-0896(97)00170-3