N,N-dimethylaniline/boron tribromide 1:1 complex

Base Information

Chemical Name:N,N-dimethylaniline/boron tribromide 1:1 complex
CAS No.:17900-45-7
Molecular Formula:C₈H₁₁BBr₃N
Molecular Weight:371.705
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethylaniline/boron tribromide 1:1 complex

Chemical Property:

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Technology Process of N,N-dimethylaniline/boron tribromide 1:1 complex

There total 3 articles about N,N-dimethylaniline/boron tribromide 1:1 complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10294-33-4
boron tribromide

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 17900-45-7
N,N-dimethylaniline/boron tribromide 1:1 complex

Guidance literature:: In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tetlet.2016.07.017

Reference yield:

: 7637-07-2
boron trifluoride

: 10294-33-4
boron tribromide

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 17900-45-7
N,N-dimethylaniline/boron tribromide 1:1 complex

: 82862-34-8
N,N-dimethylaniline

: 455-28-7
N,N-dimethylaniline*BF₃

: 82862-35-9
N,N-dimethylaniline*BFBr₂

Guidance literature:: In chloroform-d1; excess of BBr3 dissolved in dry CDCl3 under N2, added to amine-BF3 soln., excess of amine added or equilibrated mixt. of BF3 and BBr3 added to soln. of amine in dry CDCl3, frozen, degassed in vac.; without isolation;

Reference yield:

: 7637-07-2
boron trifluoride

: 10294-33-4
boron tribromide

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 17900-45-7
N,N-dimethylaniline/boron tribromide 1:1 complex

: N,N-dimethylaniline*BCl₂Br

: N,N-dimethylaniline*BClBr₂

: 34321-70-5
N,N-dimethylaniline*BCl₃

Guidance literature:: In chloroform-d1; equilibrated mixt. of BCl3 and BBr3 added to soln. of amine in dry CDCl3, frozen, degassed in vac.; without isolation;