C₂₇H₄₅BN₂O₆

Base Information

Chemical Name:C₂₇H₄₅BN₂O₆
CAS No.:1428265-92-2
Molecular Formula:C₂₇H₄₅BN₂O₆
Molecular Weight:504.475
Hs Code.:

C<sub>27</sub>H<sub>45</sub>BN<sub>2</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₄₅BN₂O₆

Chemical Property:

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Technology Process of C₂₇H₄₅BN₂O₆

There total 9 articles about C₂₇H₄₅BN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345673-10-0
ethyl 2-(tert-butoxycarbonylamino)-2-formyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

: 100-46-9
benzylamine

: 1428265-92-2
C₂₇H₄₅BN₂O₆

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 60 ℃; for 2h;
DOI:10.1016/j.bmcl.2013.02.024

Reference yield:

: 102831-44-7
diethyl tert-butoxycarbonylaminomalonate

: 1428265-92-2
C₂₇H₄₅BN₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1: sodium hydride / N,N-dimethyl-formamide / 90 °C

2: potassium hydroxide / ethanol / 19 h / 0 - 20 °C

3: triethylamine

4: sodium tetrahydroborate / 1 h / -40 °C

5: dmap / dichloromethane / 16 h / 20 °C

6: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 10 h / 20 °C

7: potassium carbonate / ethanol / 2 h / 20 °C

8: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

9: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 2 h / 60 °C

With dmap; sodium tetrahydroborate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; oxalyl dichloride; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; 1,2-bis-(diphenylphosphino)ethane; potassium hydroxide; In ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.02.024

Reference yield:

: diethyl 2-but-3-enyl-2-(tert-butoxycarbonylamino)propanedioate

: 1428265-92-2
C₂₇H₄₅BN₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1: potassium hydroxide / ethanol / 19 h / 0 - 20 °C

2: triethylamine

3: sodium tetrahydroborate / 1 h / -40 °C

4: dmap / dichloromethane / 16 h / 20 °C

5: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 10 h / 20 °C

6: potassium carbonate / ethanol / 2 h / 20 °C

7: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

8: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 2 h / 60 °C

With dmap; sodium tetrahydroborate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; oxalyl dichloride; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; dimethyl sulfoxide; triethylamine; 1,2-bis-(diphenylphosphino)ethane; potassium hydroxide; In ethanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2013.02.024