tri-p-tolyl-triphenyldiplumbane

Base Information

Chemical Name:tri-p-tolyl-triphenyldiplumbane
CAS No.:104026-61-1
Molecular Formula:C₃₉H₃₆Pb₂
Molecular Weight:919.115
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri-p-tolyl-triphenyldiplumbane

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Technology Process of tri-p-tolyl-triphenyldiplumbane

There total 1 articles about tri-p-tolyl-triphenyldiplumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1802-69-3
(triphenylplumbyl)lithium

: 104026-67-7
(C₆H₄CH₃)3PbCl

: 104026-69-9,104026-61-1
tri-p-tolyl-triphenyldiplumbane

Guidance literature:: In tetrahydrofuran; byproducts: C6H6; dropwise addn. of Ph3PbLi to (p-tol)3PbCl (-60°C, during 10 min), stirring (2 h, warming to 20°C); addn. of cold MeOH (pptn.), repptn. (benzene/MeOH or CHCl3/MeOH); elem.anal.;
DOI:10.1016/0022-328X(85)80302-8