C₁₆H₂₁⁽²⁾H₂NO

Base Information

Chemical Name:C₁₆H₂₁⁽²⁾H₂NO
CAS No.:1352167-38-4
Molecular Formula:C₁₆H₂₃NO
Molecular Weight:247.349
Hs Code.:

C<sub>16</sub>H<sub>21</sub><sup>(2)</sup>H<sub>2</sub>NO

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₁⁽²⁾H₂NO

Chemical Property:

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Technology Process of C₁₆H₂₁⁽²⁾H₂NO

There total 5 articles about C₁₆H₂₁⁽²⁾H₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₁⁽²⁾H₂NO

: C₁₆H₂₁⁽²⁾H₂NO

: 1352167-38-4
C₁₆H₂₁⁽²⁾H₂NO

Guidance literature:: With Et₃PAuNTf₂; In dichloromethane; at 0 ℃; for 6h; Molecular sieve; Inert atmosphere;
DOI:10.1021/ja208860x

Reference yield:

: 1352167-46-4
C₁₁H₁₅⁽²⁾H₂N

: C₁₆H₂₁⁽²⁾H₂NO

: 1352167-38-4
C₁₆H₂₁⁽²⁾H₂NO

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; sodium iodide / acetonitrile / 12 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Molecular sieve; Inert atmosphere

3: Et₃PAuNTf₂ / dichloromethane / 6 h / 0 °C / Molecular sieve; Inert atmosphere

With Et₃PAuNTf₂; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1021/ja208860x

Reference yield:

: 1352167-37-3
C₁₆H₂₁⁽²⁾H₂N

: C₁₆H₂₁⁽²⁾H₂NO

: 1352167-38-4
C₁₆H₂₁⁽²⁾H₂NO

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C / Molecular sieve; Inert atmosphere

2: Et₃PAuNTf₂ / dichloromethane / 6 h / 0 °C / Molecular sieve; Inert atmosphere

With Et₃PAuNTf₂; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja208860x