methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

Base Information

Chemical Name:methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate
CAS No.:1234501-75-7
Molecular Formula:C₅₈H₁₀₆O₈Si₃
Molecular Weight:1015.73
Hs Code.:

methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

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Chemical Property of methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

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Technology Process of methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

There total 1 articles about methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.7%

: 1075200-47-3
C₁₇H₃₀O₄Si

: 1234500-98-1
1-[3R,9R-bis-(tert-butyldimethylsilanyloxy)-12-iodo-2R,8S,10S-trimethyl-1S-(1S-methylpent-2Z-enyl)-dodec-11Z-enyloxymethyl]-4-methoxybenzene

: 1234501-25-7
1S-[3R,9R-bis-(tert-butyldimethylsilanyloxy)-2R,8S,10S-trimethyl-1-(1S-methylpent-2Z-enyl)-dodec-11-enyloxymethyl]-4-methoxybenzene

: 1234501-75-7
methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9R-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

: 1234501-24-6
methyl 7S,13R,19R-tris(tert-butyldimethylsilanyloxy)-9S-hydroxy-21S-(4-methoxy-benzyloxy)-6S,12S,14S,20R,22S-pentamethylhexacosa-2Z,4E,10Z,23Z-tetraenoate

Guidance literature:: 1-[3R,9R-bis-(tert-butyldimethylsilanyloxy)-12-iodo-2R,8S,10S-trimethyl-1S-(1S-methylpent-2Z-enyl)-dodec-11Z-enyloxymethyl]-4-methoxybenzene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃; for 0.5h; Inert atmosphere;

C₁₇H₃₀O₄Si; In diethyl ether; pentane; at -78 ℃; Inert atmosphere;

With ammonium chloride; In diethyl ether; pentane; Inert atmosphere;
DOI:10.1021/ja103537u