Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)

Base Information

Chemical Name:Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)
CAS No.:1250872-09-3
Molecular Formula:C₅₆H₅₄BrMnN₂OP₄
Molecular Weight:1029.79
Hs Code.:

Synonyms:

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Chemical Property of Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)

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Technology Process of Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)

There total 1 articles about Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1250872-04-8
Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(CO)3(Br)

: 2071-20-7
bis-diphenylphosphinomethane

: 1250872-09-3
Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)

Guidance literature:: In fluorobenzene; Irradiation (UV/VIS); (N2) mixt. Mn complex and ligand in PhF was photolyzed using Ace Hanovia450 W medium pressure Hg lamp for 4-6 h; soln. was evapd. in vacuo, residue was dissolved in THF, hexane was added, stirred overnight, ppt. was filtered and dried in vacuo;
DOI:10.1021/om100668e

Reference yield: 99.0%

: 16853-85-3
lithium aluminium tetrahydride

: 1250872-09-3
Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(Br)

: 1250872-12-8
Mn(1,5-diphenyl-3,7-dibenzyl-1,5-diaza-3,7-diphosphacyclooctane)(bis(diphenylphosphino)methane)(CO)(H)

Guidance literature:: In tetrahydrofuran; (N2) LiAlH4 was added to soln. Mn complex in THF and stirred for 16 h; soln. was filtered through Celite, water was added, soln. was filtered through Celite and evapd. in vacuo; elem. anal.;
DOI:10.1021/om100668e