B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4]

Base Information

• Chemical Name: B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4]
• CAS No.: 1287239-92-2
• Molecular Formula: C₇H₁₃N₂*C₂₉H₄₀BN₂O
• Molecular Weight: 568.654
• Mol file: 1287239-92-2.mol

Synonyms:

Chemical Property of B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4]

There total 4 articles about B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1,3,4,5-tetramethylimidazol-2-ylidine (256238-51-4) + borinic acid (1287239-90-0) → B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2(1-)*N2C3H(CH3)4(1+)=[B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2][N2C3H(CH3)4] (1287239-92-2)

Guidance literature:

In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201007417

Reference yield:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) → B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2(1-)*N2C3H(CH3)4(1+)=[B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2][N2C3H(CH3)4] (1287239-92-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / -78 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: water; 1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene / toluene / 20 °C / Inert atmosphere

3.1: toluene / 20 °C / Inert atmosphere

With n-butyllithium; water; 1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene; In diethyl ether; hexane; toluene;

DOI:10.1002/anie.201007417

Reference yield:

((CH(CH3)2)2C6H3N)2CCH2CHCCH3BBr (1287239-89-7) → B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2(1-)*N2C3H(CH3)4(1+)=[B(O)N2C3H(CH3)(CH2)(C6H3(CH(CH3)2)2)2][N2C3H(CH3)4] (1287239-92-2)

Guidance literature:

Multi-step reaction with 2 steps

1: water; 1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene / toluene / 20 °C / Inert atmosphere

2: toluene / 20 °C / Inert atmosphere

With water; 1,3-diisopropyl-4,5-dimethyl-1H-imidazol-2(3H)-ylidene; In toluene;

DOI:10.1002/anie.201007417

upstream raw materials:

borinic acid

1,3,4,5-Tetramethylimidazol-2-yliden

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

1,3,4,5-tetramethylimidazol-2-ylidine