C₃₀H₃₃ClO₉

Base Information

Chemical Name:C₃₀H₃₃ClO₉
CAS No.:1185339-54-1
Molecular Formula:C₃₀H₃₃ClO₉
Molecular Weight:573.04
Hs Code.:

C<sub>30</sub>H<sub>33</sub>ClO<sub>9</sub>

Synonyms:

Suppliers and Price of C₃₀H₃₃ClO₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₃ClO₉

Chemical Property:

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Technology Process of C₃₀H₃₃ClO₉

There total 12 articles about C₃₀H₃₃ClO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-11-6
diiodomethane

: 1185339-52-9
C₂₉H₃₁ClO₉

: 1185339-54-1
C₃₀H₃₃ClO₉

Guidance literature:: With diethylzinc; trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 1185339-44-9
C₁₉H₂₁ClO₅

: 1185339-54-1
C₃₀H₃₃ClO₉

Guidance literature:: Multi-step reaction with 5 steps

1: dmap / pyridine; dichloromethane / 20 °C

2: aluminum (III) chloride / dichloromethane / 0 - 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

4: toluene-4-sulfonic acid / water; toluene / Reflux

5: diethylzinc; trifluoroacetic acid / dichloromethane / 0 - 20 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; diethylzinc; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; toluene; 2: Friedel Crafts acylation / 5: Simmons-Smith reaction;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 312749-31-8
2-chloro-5-bromobenzophenone

: 1185339-54-1
C₃₀H₃₃ClO₉

Guidance literature:: Multi-step reaction with 9 steps

1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux

2: n-butyllithium / tetrahydrofuran; toluene / -78 °C

3: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C

4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C

5: dmap / pyridine; dichloromethane / 20 °C

6: aluminum (III) chloride / dichloromethane / 0 - 20 °C

7: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

8: toluene-4-sulfonic acid / water; toluene / Reflux

9: diethylzinc; trifluoroacetic acid / dichloromethane / 0 - 20 °C

With triethylsilane; dmap; aluminum (III) chloride; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; diethylzinc; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; methanesulfonic acid; dichloromethane; water; toluene; acetonitrile; 6: Friedel Crafts acylation / 9: Simmons-Smith reaction;
DOI:10.1016/j.bmcl.2011.06.032