N,N-dimethylethylamine

Base Information

Chemical Name: N,N-dimethylethylamine
CAS No.:81224-29-5
Molecular Formula:C₂₀H₂₁ClN₂O₂
Molecular Weight:356.852
Hs Code.:

<p-chlorobenzoyl-7 methoxy-4 indolyl-1> N,N-dimethylethylamine

Synonyms:

Suppliers and Price of N,N-dimethylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethylethylamine

Chemical Property:

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Technology Process of N,N-dimethylethylamine

There total 8 articles about N,N-dimethylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-57-4
2-bromoanisole

: 81224-29-5
N,N-dimethylethylamine

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / AlCl₃ / CH₂Cl₂ / 0.33 h / 0 °C

2: 88 percent / p-TsOH / benzene / 40 h / Heating

3: 1) n-BuLi / 1) ether, -20 deg C, 4 h , 2) RT, 12 h

4: CH₃ONa / methanol / 5 h / 0 °C

5: xylene / 3 h / Heating

6: 93 percent / aq. KOH / 0.5 h / Heating

7: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

8: 1) NaH / 1) DMF, 0 deg C, 30 min, 2) 100 deg C, 2 h

With n-butyllithium; aluminium trichloride; sodium methylate; sodium hydride; toluene-4-sulfonic acid; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; dichloromethane; xylene; benzene;

Reference yield:

: 81224-20-6
(3-bromo-4-methoxyphenyl)(4-chlorophenyl)methanone

: 81224-29-5
N,N-dimethylethylamine

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / p-TsOH / benzene / 40 h / Heating

2: 1) n-BuLi / 1) ether, -20 deg C, 4 h , 2) RT, 12 h

3: CH₃ONa / methanol / 5 h / 0 °C

4: xylene / 3 h / Heating

5: 93 percent / aq. KOH / 0.5 h / Heating

6: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

7: 1) NaH / 1) DMF, 0 deg C, 30 min, 2) 100 deg C, 2 h

With n-butyllithium; sodium methylate; sodium hydride; toluene-4-sulfonic acid; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene; benzene;

Reference yield:

: 81224-22-8
p-chlorobenzoyl-5 methoxy-2 benzaldehyde

: 81224-29-5
N,N-dimethylethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: CH₃ONa / methanol / 5 h / 0 °C

2: xylene / 3 h / Heating

3: 93 percent / aq. KOH / 0.5 h / Heating

4: 77 percent / copper chromite (barium promoted) / quinoline / 7 h / 190 °C

5: 1) NaH / 1) DMF, 0 deg C, 30 min, 2) 100 deg C, 2 h

With sodium methylate; sodium hydride; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene;