(2S,6R)-2--6-methyl-1,3-dioxan-4-one

Base Information

Chemical Name:(2S,6R)-2--6-methyl-1,3-dioxan-4-one
CAS No.:139764-53-7
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

(2S,6R)-2-<benzyloxymethyl>-6-methyl-1,3-dioxan-4-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,6R)-2--6-methyl-1,3-dioxan-4-one

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Technology Process of (2S,6R)-2--6-methyl-1,3-dioxan-4-one

There total 3 articles about (2S,6R)-2--6-methyl-1,3-dioxan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19810-31-2
Benzyloxyacetyl chloride

: 139764-53-7
(2S,6R)-2--6-methyl-1,3-dioxan-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂ / Ambient temperature

2: 67 percent / DIBAL / diethyl ether / 0.5 h / -78 °C

3: PPTS / CH₂Cl₂ / 66 h / Heating

With pyridine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)80578-0

Reference yield:

: 31600-43-8
methyl 2-(benzyloxy)acetate

: 139764-53-7
(2S,6R)-2--6-methyl-1,3-dioxan-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / DIBAL / diethyl ether / 0.5 h / -78 °C

2: PPTS / CH₂Cl₂ / 66 h / Heating

With pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)80578-0

Reference yield:

: 625-72-9,26063-00-3,29435-48-1
(R)-3-hydroxybutyric acid

: 60656-87-3
benzyloxyacetoaldehyde

: 131991-73-6
(2R,6R)-2--6-methyl-1,3-dioxan-4-one

: 139764-53-7
(2S,6R)-2--6-methyl-1,3-dioxan-4-one

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 66h; Yield given. Yields of byproduct given; Heating;
DOI:10.1016/S0040-4020(01)80578-0