[(n-Bu)2Sn(H₂O)(1,10-phenanthroline)(O₃SC₆H₃-2,5-Me₂)][2,5-Me₂C₆H₃SO₃]

Base Information

• Chemical Name: [(n-Bu)2Sn(H₂O)(1,10-phenanthroline)(O₃SC₆H₃-2,5-Me₂)][2,5-Me₂C₆H₃SO₃]
• CAS No.: 941303-42-0
• Molecular Formula: C₈H₉O₃S*C₂₈H₃₇N₂O₄SSn
• Molecular Weight: 801.612
• Mol file: 941303-42-0.mol

Synonyms:

Chemical Property of [(n-Bu)2Sn(H₂O)(1,10-phenanthroline)(O₃SC₆H₃-2,5-Me₂)][2,5-Me₂C₆H₃SO₃]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(n-Bu)2Sn(H₂O)(1,10-phenanthroline)(O₃SC₆H₃-2,5-Me₂)][2,5-Me₂C₆H₃SO₃]

There total 1 articles about [(n-Bu)2Sn(H₂O)(1,10-phenanthroline)(O₃SC₆H₃-2,5-Me₂)][2,5-Me₂C₆H₃SO₃] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,10-Phenanthroline (66-71-7) + [(n-Bu)2Sn(H2O)4][2,5-Me2C6H3SO3]2 → [(n-Bu)2Sn(H2O)(1,10-phenanthroline)(O3SC6H3-2,5-Me2)][2,5-Me2C6H3SO3] (941303-42-0)

Guidance literature:

In toluene; suspn. of Sn complex and ligand in toluene was stirred at 60°c for 15 h; filtered; slowly evapd. for 5 d; elem. anal.;

DOI:10.1021/om0701625

Reference yield:

[(n-Bu)2Sn(H2O)(1,10-phenanthroline)(O3SC6H3-2,5-Me2)][2,5-Me2C6H3SO3] (941303-42-0) → [(n-Bu)2Sn(μ-OH)(2,5-Me2C6H3SO3)]2

Guidance literature:

With pyridine; In toluene; mixt. of pyridine and Sn compd. in toluene was heated at 60°C overnight;

DOI:10.1021/om0701625

Reference yield:

[(n-Bu)2Sn(H2O)(1,10-phenanthroline)(O3SC6H3-2,5-Me2)][2,5-Me2C6H3SO3] (941303-42-0) + water (7732-18-5) → [(n-Bu)2Sn(μ-OH)(2,5-Me2C6H3SO3)]2

Guidance literature:

With pyridine; In toluene; pyridine was added to suspn. of Sn complex in toluene; mixt. was stirredat 60°C overnight; solvent removed; dissolved in MeOH; slowly evapd.;

DOI:10.1021/om0701625

upstream raw materials:

1,10-Phenanthroline