4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

Base Information

Chemical Name:4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃
CAS No.:114306-60-4
Molecular Formula:C₂₂H₁₉O₃Sb
Molecular Weight:453.141
Hs Code.:

4-C<sub>2</sub>H<sub>5</sub>OOC<sub>6</sub>H<sub>4</sub>SbC<sub>12</sub>H<sub>7</sub>OCH<sub>3</sub>

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Chemical Property of 4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

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Technology Process of 4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

There total 5 articles about 4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 855884-99-0
{2-(4-CH₃OC₆H₄C₆H₄)}(4-C₂H₅OOCC₆H₄)SbCl₃

: 114306-60-4
4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

Guidance literature:: With sodium acetate; stannous chloride; In acetone; addn. of aq. sodium acetate to Sb-compd., pptd. stibinic acid cyclized by dehydration in acetic anhydride contg. H2SO4; the crude stibafluorene oxide is reduced by stannous chloride in acetone; recrystn. from ethyl acetate/ethanol;
DOI:10.1039/JR9550001662

Reference yield:

: (3-CH₃O-6-C₆H₅C₆H₃)(4-C₂H₅OOCC₆H₄)SbCl₃

: 114306-60-4
4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

Guidance literature:: With sodium acetate; stannous chloride; In acetone; addn. of aq. sodium acetate to Sb-compd., pptd. stibinic acid cyclized by dehydration in acetic anhydride contg. H2SO4; the crude stibafluorene oxide is reduced by stannous chloride in acetone; recrystn. from ethyl acetate/ethanol;
DOI:10.1039/JR9550001662

Reference yield:

: 855199-49-4
4-C₂H₅O₂CC₆H₄SbCl₂

: 114306-60-4
4-C₂H₅OOC₆H₄SbC₁₂H₇OCH₃

Guidance literature:: Multi-step reaction with 2 steps

1: Cu bronze / ethanol

2: sodium acetate; stannous chloride / acetone

With Cu bronze; sodium acetate; stannous chloride; In ethanol; acetone;
DOI:10.1039/JR9550001662